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41.
《Ceramics International》2020,46(10):16088-16095
The Pechini-type sol-gel (PSG) process has been used for the preparation of doped oxides due to its capability to overcome most of the difficulties that frequently occur by using other producing methods. In this work we analyze the case of samples of pure and In-doped yttria (Y2O3) prepared by the PSG process. We experimentally characterize the synthesized samples by x-ray diffraction, micro-Raman spectroscopy, electrochemical impedance spectroscopy (EIS), and time-differential perturbed γ-γ angular correlation (PAC) spectroscopy, and we compare these results with those obtained starting from commercial oxide powders. We found that the PSG process can be used to successfully produce doped yttria in the cubic phase, with the impurities substitutionally located at the cationic sites of the structure. By the proposed PSG route, the inclusion of impurities does not affect the particle size nor the resistivity. However, when we compare the PSG samples with other samples produced from commercial powder, we found that the first have lower resistivities at grain interiors. On the other hand, PAC spectroscopy in 111In(→111Cd)-doped yttria allows the study of the dynamic hyperfine interactions observed by the radioactive 111Cd impurity-probe, which can be used to “sense” the host electron availability near the impurities after the electron-capture decay of 111In. Differences between PAC spectra for PSG samples and the commercial powder suggest that the PSG process introduces additional donor defects into the yttria electronic structure, which is consistent with the lower resistivity observed in the PSG samples by EIS spectroscopy. 相似文献
42.
在煤矿测量工作中,贯通测量是其中重要工作之一,确保贯通点的误差在设定的范围内,决定了贯通测量的成败。本文将马脊梁煤矿副立井与王村回风立井的贯通作为研究对象,选择使用井下控制测量、竖井联系测量及陀螺定向技术等,设定了贯通测量的方案,开展了误差预计,通过对比预计结果和要求,保证了贯通测量设计的可行性。 相似文献
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为保障煤矿安全开采,有针对性地制定预防和治理措施,对红石岩煤矿隐蔽致灾因素进行探究。首先梳理了红石岩煤矿已揭露的地质情况和现有的钻探、物探和水质化验成果,瓦斯鉴定等资料,结合煤矿隐蔽致灾因素具有隐蔽性、时变性、突发性、难探测和难预防的特点,对其地面和井田内的采空区、废弃老窑,钻孔、地质构造、地下含水体、瓦斯和煤层自燃及煤层顶底板等因素进行了分析。总结出该矿主副井筒周边采空区水、因采动影响产生的顶底板导水裂隙带等主要隐蔽致灾因素,以及断层的活化和滞后出水及带出的有害气体等次要隐蔽致灾因素,并提出了相应的预防和治理措施。 相似文献
46.
采用综合应用理论分析、现场实测的方法,对山西汾西集团曙光煤矿1226高瓦斯综采工作面瓦斯来源进行了分析,提出并实施了分区段“风排+煤层钻孔抽放+裂隙带钻孔抽放”的联合瓦斯抽采技术。现场监测结果显示:1226综采工作面上隅角瓦斯浓度控制在0.45%~0.75%,回风流中瓦斯浓度控制在了0.44%~0.75%,瓦斯治理效果明显改善。 相似文献
47.
Alternative selection in new product development (NPD) is a multi-criteria decision-making (MCDM) problem. It usually starts with incomplete, imprecise or even partially missing information. Currently, most existing methods in dealing with this problem cannot work well if required information is incomplete or missing. It is acknowledged that stochastic multi-objective acceptability analysis (SMAA) can be applied to address MCDM problem with incomplete preference information and uncertain criteria measurements. In SMAA, alternatives are evaluated based on SMAA measurements (acceptability index, central weight vector and confidence factor). The discriminability of SMAA for the optimum alternative heavily depends on differences of SMAA measurements among different alternatives. Usually, a large number of alternatives and high level of uncertainty are involved in alternative selection in NPD. In this situation, the differences among SMAA measurements are not obvious, and therefore SMAA cannot deal with such problem very well. To this end, this paper proposes an improved SMAA method called Iterative-SMAA (I-SMAA) for alternative selection in NPD. In the I-SMAA, an iterative multi-step decision-making process is suggested to improve differences of SMAA measurements among different alternatives, and thus assist decision makers (DMs) to positively discern from the most preferred alternative. To enhance the decision-making efficiency, sensitive criteria are acquired in each iteration by ranking sensitivity analysis. DMs are guided to provide partial preference information and give more accurate criteria measurements for sensitive criteria rather than all criteria. Eventually, to verify the proposed method, a numerical example of the existing literature is solved with the method, and the results are compared. And then, a practical example of a preparation equipment for coal samples is further employed to verify the practicability of the proposed I-SMAA. 相似文献
48.
李力 《工业技术与职业教育》2020,18(1):50-53
"班组长型"人才正是实现"中国制造2025"宏伟蓝图的基层驱动力量之一,"班组长型"人才的培养是当前相关职业院校重要任务,分析了"中国制造2025"对当前高职教育的新挑战以及对企业班组长的新要求,并提出了"中国制造2025"背景下"班组长型"人才培养的应对措施。 相似文献
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50.
Ying Guo Mengting Ma Fan Jiang Wenqian Jiang Hanxin Wang Shuang-kui Du 《International Journal of Food Science & Technology》2020,55(2):720-728
Protein quality and antioxidant properties of soymilk derived from black soybean (eight varieties) in China were analysed following in vitro simulated gastrointestinal digestion (including dialysis). Soymilk from black soybean possessed high okara weight but low yield, protein content and sensory scores. The in vitro digestibility of protein in all black soymilk samples was higher than 60%, and the Shenmu black soybean exhibited the highest digestibility. Non-digested milk from the black soybean exhibited significantly high total phenolic content (TPC) (127.15–173.04 mg/100 mL), ferric-reducing antioxidant power (FRAP) (272.18–366.27 μmol L−1) and DPPH free radical-scavenging activity (61.20–83.81%). These parameters were significantly lower in the non-digested soymilk than those in soymilk after gastric digestion but higher than those of soymilk in the dialysed fraction. Gastric digestion significantly increased bioactive compound levels released from black soymilk, and the bioaccessibility of phenolic compounds was 24.37–36.05%. Hence, black soymilk was sufficiently available for human absorption. 相似文献